1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

Base Information

Chemical Name:1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene
CAS No.:168917-07-5
Molecular Formula:C₃₅H₄₈O₅Sn
Molecular Weight:667.473
Hs Code.:

Synonyms:1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

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Chemical Property of 1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

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Technology Process of 1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

There total 1 articles about 1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 168917-02-0
1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

: 108-24-7
acetic anhydride

: 168917-07-5
1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

Guidance literature:: With dmap; triethylamine; In dichloromethane; stirring (room temp., 17 h), concn. under reduced pressure; chromatography; elem. anal.;
DOI:10.1021/ja00117a009

Reference yield: 22.0%

: 168917-07-5
1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

: 1,4-diacetoxy-2-(1-methylethoxy)-3-phenylnaphthalene

: 2,7-bis(1-methylethoxy)-5-hydroxy-6-methyl-3-phenyl-1,4-diacetoxyphenanthrene

: 2,7-bis(1-methylethoxy)-4-hydroxy-6-methyl-3-phenyl-1,5-diacetoxyphenanthrene

: Acetic acid 5,5',8'-triacetoxy-6,6'-diisopropoxy-7,7'-diphenyl-[2,2']binaphthalenyl-8-yl ester

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; 4-Chloro-2-methyl-3-(1-methylethoxy)-2-cyclobutenone; In 1,4-dioxane; for 23h; Heating;
DOI:10.1021/ja00117a009

Reference yield:

: 108-24-7
acetic anhydride

: 138151-56-1
4-Chloro-2-methyl-3-(1-methylethoxy)-2-cyclobutenone

: 168917-07-5
1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

: 1,4-diacetoxy-2-(1-methylethoxy)-3-phenylnaphthalene

: 2,7-bis(1-methylethoxy)-6-methyl-3-phenyl-1,4,5-triacetoxyphenanthrene

: Acetic acid 5,5',8'-triacetoxy-6,6'-diisopropoxy-7,7'-diphenyl-[2,2']binaphthalenyl-8-yl ester

Guidance literature:: With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; triethylamine; Yield given. Multistep reaction. Yields of byproduct given; 1.) dioxane, reflux, 23, 2.) CH₂Cl₂, RT, 22 h;
DOI:10.1021/ja00117a009