1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

Base Information

Chemical Name:1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene
CAS No.:168917-02-0
Molecular Formula:C₃₃H₄₆O₄Sn
Molecular Weight:625.436
Hs Code.:

Synonyms:1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

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Chemical Property of 1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

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Technology Process of 1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

There total 1 articles about 1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 168916-94-7
4-acetoxy-3-(1-methylethoxy)-2-phenyl-4[4'-(tri-n-butylstannyl)-phenyl]-2-cyclobuten-1-one

: 168917-02-0
1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

Guidance literature:: In xylene; reflux 1.5 h, cooling to room temp.; chromatography; elem. anal.;
DOI:10.1021/ja00117a009

Reference yield: 96.0%

: 168917-02-0
1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

: 74-88-4
methyl iodide

: 168917-08-6
1-acetoxy-4-methoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

Guidance literature:: With potassium carbonate; In acetone; stirring (room temp., 19 h); filtration, concn. of the filtrate; chromatography; elem. anal.;
DOI:10.1021/ja00117a009

Reference yield: 95.0%

: 168917-02-0
1-acetoxy-4-hydroxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

: 108-24-7
acetic anhydride

: 168917-07-5
1,4-diacetoxy-2-(1-methylethoxy)-3-phenyl-6-(tri-n-butylstannyl)naphthalene

Guidance literature:: With dmap; triethylamine; In dichloromethane; stirring (room temp., 17 h), concn. under reduced pressure; chromatography; elem. anal.;
DOI:10.1021/ja00117a009