4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

Base Information

Chemical Name:4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide
CAS No.:1235562-92-1
Molecular Formula:C₁₅H₉Br₂F₃N₂O₃
Molecular Weight:482.051
Hs Code.:

Synonyms:4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

Chemical Property:

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Technology Process of 4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

There total 3 articles about 4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 175277-18-6
4-trifluoromethoxybenzoyl hydrazine

: 90-59-5
3,5-Dibromosalicylaldehyde

: 1235562-92-1
4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

Guidance literature:: With acetic acid; In methanol; at 20 ℃;
DOI:10.1021/acs.jmedchem.9b01004

Reference yield:

: 780-31-4
methyl 4-(trifluoromethoxy)benzoate

: 1235562-92-1
4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / Reflux

2: acetic acid / methanol / 20 °C

With hydrazine hydrate; acetic acid; In methanol;
DOI:10.1021/acs.jmedchem.9b01004

Reference yield:

: 330-12-1
4-trifluoromethoxybenzoic acid

: 1235562-92-1
4-trifluoromethoxy-N'-(3,5-dibromo-2-hydroxybenzylidene)benzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / Reflux

2: hydrazine hydrate / methanol / Reflux

3: acetic acid / methanol / 20 °C

With sulfuric acid; hydrazine hydrate; acetic acid; In methanol;
DOI:10.1021/acs.jmedchem.9b01004