CH₂CHC₆H₄BBr₂

Base Information

• Chemical Name: CH₂CHC₆H₄BBr₂
• CAS No.: 1082577-48-7
• Molecular Formula: C₈H₇BBr₂
• Molecular Weight: 273.763
• Mol file: 1082577-48-7.mol

Synonyms:CH₂CHC₆H₄BBr₂

Chemical Property of CH₂CHC₆H₄BBr₂

Chemical Property:

Purity/Quality:

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Technology Process of CH₂CHC₆H₄BBr₂

There total 1 articles about CH₂CHC₆H₄BBr₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

4-(trimethylsilyl)styrene (1009-43-4) + boron tribromide (10294-33-4) → CH2CHC6H4BBr2 (1082577-48-7)

Guidance literature:

In dichloromethane; byproducts: (CH3)3SiBr; Si-polymer treated with excess of BBr3; pptd. into hexane;

DOI:10.1021/ja020773i

Reference yield: 90.0%

ethyl trimethylsilyl ether (1825-62-3) + CH2CHC6H4BBr2 (1082577-48-7) → diethoxy-(4-vinyl-phenyl)-borane (14559-99-0)

Guidance literature:

In not given; freeze-dried from benzene;

DOI:10.1021/ja020773i

Reference yield: 83.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + CH2CHC6H4BBr2 (1082577-48-7) → CH2CHC6H4B(OC4H8Br)2

Guidance literature:

In not given; pptd. into hexane;

DOI:10.1021/ja020773i

upstream raw materials:

4-(trimethylsilyl)styrene

boron tribromide

Downstream raw materials:

diethoxy-(4-vinyl-phenyl)-borane

t-BuC₆H₄(St)BBr

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)styrene