N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

Base Information

Chemical Name:N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester
CAS No.:84941-57-1
Molecular Formula:C₂₂H₂₈N₂O₃
Molecular Weight:368.476
Hs Code.:

Synonyms:N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

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Chemical Property of N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

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Technology Process of N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

There total 3 articles about N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 107-21-1
ethylene glycol

: 84941-56-0
1,1-Diphenyl-2-piperidino-ethyl-isocyanat

: 84941-57-1
N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

Guidance literature:: With potassium hydroxide; at 120 ℃; for 1h;
DOI:10.1002/ardp.19833160111

Reference yield:

: 63326-31-8
α,α-Diphenyl-β-piperidino-propionsaeureamid

: 84941-57-1
N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Br₂, NaOH / 2 h

2: 74 percent / KOH / 1 h / 120 °C

With potassium hydroxide; sodium hydroxide; bromine;
DOI:10.1002/ardp.19833160111

Reference yield:

: 857385-60-5
α,α-Diphenyl-β-piperidino-propionitril

: 84941-57-1
N-(1,1-Diphenyl-2-piperidino-ethyl)-carbamidsaeure-(2-hydroxyethyl)ester

Guidance literature:: Multi-step reaction with 3 steps

1: conc. H₂SO₄

2: 75 percent / Br₂, NaOH / 2 h

3: 74 percent / KOH / 1 h / 120 °C

With potassium hydroxide; sodium hydroxide; sulfuric acid; bromine;
DOI:10.1002/ardp.19833160111