Technology Process of C30H51N5O7S
There total 10 articles about C30H51N5O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
di-tert-butyl dicarbonate;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 25 ℃;
for 0.25h;
C16H32N4O2;
In
dichloromethane; N,N-dimethyl-formamide;
at 25 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetic acid / methanol / 1 h / 20 °C
1.2: Cooling with ice
2.1: lithium aluminium tetrahydride; sulfuric acid / tetrahydrofuran / 0 - 50 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C
4.1: hydrogen / palladium(II) hydroxide / methanol / 16 h
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 25 °C
5.2: 16 h / 25 °C
With
lithium aluminium tetrahydride; sulfuric acid; hydrogen; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
palladium(II) hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride; sulfuric acid / tetrahydrofuran / 0 - 50 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 25 °C
3.1: hydrogen / palladium(II) hydroxide / methanol / 16 h
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 25 °C
4.2: 16 h / 25 °C
With
lithium aluminium tetrahydride; sulfuric acid; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
palladium(II) hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;