6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

Base Information

Chemical Name:6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene
CAS No.:909266-35-9
Molecular Formula:C₂₀H₁₇N₇O₄
Molecular Weight:419.399
Hs Code.:

Synonyms:6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

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Chemical Property of 6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

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Technology Process of 6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

There total 3 articles about 6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 909266-32-6
6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-4'-methoxy-2,4-dinitrostilbene

: 909266-35-9
6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1007/s11172-005-0403-4

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 909266-35-9
6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Et₃N / ethanol / 80 °C

2: 81 percent / NaN₃ / dimethylformamide / 4 h / 20 °C

With sodium azide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/s11172-005-0403-4

Reference yield:

: 909266-29-1
1-Azido-2-[(E)-2-(4-methoxy-phenyl)-vinyl]-3,5-dinitro-benzene

: 909266-35-9
6-(4-acetyl-5-methyl-1H-1,2,3-triazol-1-yl)-2-azido-4'-methoxy-4-nitrostilbene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Et₃N / ethanol / 80 °C

2: 81 percent / NaN₃ / dimethylformamide / 4 h / 20 °C

With sodium azide; triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1007/s11172-005-0403-4