potassium hepta-1,6-diyn-1-yltrifluoroborate

Base Information

Chemical Name:potassium hepta-1,6-diyn-1-yltrifluoroborate
CAS No.:1023357-05-2
Molecular Formula:C₇H₇BF₃*K
Molecular Weight:198.037
Hs Code.:

Synonyms:potassium hepta-1,6-diyn-1-yltrifluoroborate

Suppliers and Price of potassium hepta-1,6-diyn-1-yltrifluoroborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of potassium hepta-1,6-diyn-1-yltrifluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of potassium hepta-1,6-diyn-1-yltrifluoroborate

There total 3 articles about potassium hepta-1,6-diyn-1-yltrifluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: potassium hydrogen difluoride

: 121-43-7,63156-11-6
Trimethyl borate

: 2396-63-6
hepta-1,6-diyne

: 1023357-05-2
potassium hepta-1,6-diyn-1-yltrifluoroborate

Guidance literature:: hepta-1,6-diyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; hexane; at -78 - -20 ℃; for 1h; Inert atmosphere;

potassium hydrogen difluoride; In tetrahydrofuran; hexane; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02394

Reference yield:

: 2396-63-6
hepta-1,6-diyne

: 1023357-05-2
potassium hepta-1,6-diyn-1-yltrifluoroborate

Guidance literature:: hepta-1,6-diyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

With Trimethyl borate; In tetrahydrofuran; hexane; at -78 - -20 ℃;

With potassium hydrogen bifluoride; In tetrahydrofuran; hexane; at -20 - 20 ℃; Further stages.;
DOI:10.1016/j.tetlet.2008.02.083

Reference yield:

: 1279123-63-5
potassium hydrogenfluoride

: 121-43-7,63156-11-6
Trimethyl borate

: 2396-63-6
hepta-1,6-diyne

: 1023357-05-2
potassium hepta-1,6-diyn-1-yltrifluoroborate

Guidance literature:: Trimethyl borate; hepta-1,6-diyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -20 ℃;

potassium hydrogenfluoride; In tetrahydrofuran; hexane; water; at -20 - 20 ℃; for 2h;
DOI:10.1021/jacs.8b08592