(E)-1-(4-methoxybenzyl)-2-styrylpiperidine

Base Information

Chemical Name:(E)-1-(4-methoxybenzyl)-2-styrylpiperidine
CAS No.:1380100-01-5
Molecular Formula:C₂₁H₂₅NO
Molecular Weight:307.436
Hs Code.:

Synonyms:(E)-1-(4-methoxybenzyl)-2-styrylpiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(4-methoxybenzyl)-2-styrylpiperidine

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Technology Process of (E)-1-(4-methoxybenzyl)-2-styrylpiperidine

There total 4 articles about (E)-1-(4-methoxybenzyl)-2-styrylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.1%

: 1666-17-7
benzaldehyde p-toluenesulfonylhydrazone

: 1380099-93-3
(E)-6-iodo-N-(4-methoxybenzyl)hex-5-en-1-amine

: 1380100-01-5
(E)-1-(4-methoxybenzyl)-2-styrylpiperidine

Guidance literature:: benzaldehyde p-toluenesulfonylhydrazone; With N-benzyl-N,N,N-triethylammonium chloride; lithium tert-butoxide; Inert atmosphere;

(E)-6-iodo-N-(4-methoxybenzyl)hex-5-en-1-amine; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triethylamine; triphenylphosphine; In 2-methyltetrahydrofuran; at 85 ℃; Inert atmosphere;
DOI:10.1021/ol301385g

Reference yield:

: 1-[N-(4-methoxybenzyl)amino]-5-hexyne

: 1380100-01-5
(E)-1-(4-methoxybenzyl)-2-styrylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h / -78 - 20 °C / Inert atmosphere

2.1: N-benzyl-N,N,N-triethylammonium chloride; lithium tert-butoxide / Inert atmosphere

2.2: 85 °C / Inert atmosphere

With zirconocene dichloride; N-benzyl-N,N,N-triethylammonium chloride; diisobutylaluminium hydride; lithium tert-butoxide; In tetrahydrofuran;
DOI:10.1021/ol301385g

Reference yield:

: 79496-61-0
hex-5-ynyl methanesulphonate

: 1380100-01-5
(E)-1-(4-methoxybenzyl)-2-styrylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide / dimethyl sulfoxide / 55 °C / Inert atmosphere

2.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 1 h / -78 - 20 °C / Inert atmosphere

3.1: N-benzyl-N,N,N-triethylammonium chloride; lithium tert-butoxide / Inert atmosphere

3.2: 85 °C / Inert atmosphere

With zirconocene dichloride; N-benzyl-N,N,N-triethylammonium chloride; diisobutylaluminium hydride; sodium iodide; lithium tert-butoxide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ol301385g