[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]ClO₄

Base Information

• Chemical Name: [Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]ClO₄
• CAS No.: 84190-85-2
• Molecular Formula: C₄₄H₄₂O₂P₂Rh*ClO₄
• Molecular Weight: 867.12

Synonyms:[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]ClO₄

Chemical Property of [Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]ClO₄

Chemical Property:

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Technology Process of [Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]ClO₄

There total 3 articles about [Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium (12092-47-6) + silver perchlorate + Triphenylphosphine oxide (791-28-6) → [Rh((CHCHC2H4)2)(OP(C6H5)3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OP(C6H5)3)2]ClO4 (84190-85-2)

Guidance literature:

In acetone; byproducts: AgCl; complex treated with AgClO4 in acetone, filtered, ligand added at room temp.; evapd. (vac.), suspended in hexane, filtered off, washed with hexane, air-dried; elem. anal.;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

Triphenylphosphine oxide (791-28-6) → [Rh((CHCHC2H4)2)(OP(C6H5)3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OP(C6H5)3)2]ClO4 (84190-85-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (CH₃)2CO / acetone

2: not given

With (CH₃)2CO; In acetone;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

[Rh(CO)2(OP(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)2(OP(C6H5)3)2]ClO4 (84191-03-7) + cyclo-octa-1,5-diene (5259-72-3,10060-40-9,111-78-4) → [Rh((CHCHC2H4)2)(OP(C6H5)3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OP(C6H5)3)2]ClO4 (84190-85-2)

Guidance literature:

In not given;

DOI:10.1016/S0022-328X(00)85856-8

upstream raw materials:

[Rh(CO)2(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)2(OP(C₆H₅)3)2]ClO₄

cyclo-octa-1,5-diene

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

Triphenylphosphine oxide

Downstream raw materials:

[Rh(CO)(OP(C₆H₅)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(C₆H₅)3)(P(C₆H₅)3)2]ClO₄

[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(C₆H₅)3)(P(C₆H₅)3)]ClO₄

[Rh(CO)2(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)2(OP(C₆H₅)3)2]ClO₄

[Rh(CO)(P(C₆H₅)3)(OP(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-) = [Rh(CO)(P(C₆H₅)3)(OP(C₆H₅)3)2]ClO₄

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