3'-methylacetophenone oxime acetate

Base Information

Chemical Name:3'-methylacetophenone oxime acetate
CAS No.:951682-11-4
Molecular Formula:C₁₁H₁₃NO₂
Molecular Weight:191.23
Hs Code.:

Synonyms:3'-methylacetophenone oxime acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-methylacetophenone oxime acetate

Chemical Property:

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Technology Process of 3'-methylacetophenone oxime acetate

There total 2 articles about 3'-methylacetophenone oxime acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 23040-54-2
1-m-tolyl-ethanone oxime

: 108-24-7
acetic anhydride

: 951682-11-4
3'-methylacetophenone oxime acetate

Guidance literature:: With acetic acid; at 20 ℃; for 3h;
DOI:10.1021/ol902720d

Reference yield:

: 585-74-0
3-Methylacetophenone

: 951682-11-4
3'-methylacetophenone oxime acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 100 °C

2: 3 h / 100 °C

With hydroxylamine hydrochloride; sodium acetate; In ethanol; water;
DOI:10.1039/c7cc00260b

Reference yield: 98.0%

: 951682-11-4
3'-methylacetophenone oxime acetate

: 824-79-3
sodium 4-methylbenzenesulfinate

: 1370640-77-9
2-(toluene-4-sulfonyl)-1-m-tolylethanone

Guidance literature:: 3'-methylacetophenone oxime acetate; sodium 4-methylbenzenesulfinate; With copper diacetate; In dimethyl sulfoxide; at 100 ℃; for 6h; Schlenk technique; Inert atmosphere;

With silica gel; In dichloromethane; at 20 ℃;
DOI:10.1002/anie.201311217