(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

Base Information

Chemical Name:(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone
CAS No.:1370531-40-0
Molecular Formula:C₂₄H₂₇N₃O₄S₃
Molecular Weight:517.694
Hs Code.:

Synonyms:(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

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Chemical Property of (2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

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Technology Process of (2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

There total 12 articles about (2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₉ClN₂O₄S

: 105089-88-1
(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrole

: 1370531-40-0
(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.ejmech.2012.01.014

Reference yield:

: 346723-14-6
N₁-(4-methoxyphenyl)-4-methyl-3-nitrobenzamide

: 1370531-40-0
(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

Guidance literature:: Multi-step reaction with 5 steps

1: Lawessons reagent / toluene / 60 °C / Reflux

2: Dess-Martin periodane / dichloromethane / 20 °C

3: pyridine; tetra-n-butylammonium permanganate / 12 h / 20 °C

4: thionyl chloride; N,N-dimethyl-formamide / benzene / Reflux

5: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

With Lawessons reagent; pyridine; thionyl chloride; tetra-n-butylammonium permanganate; Dess-Martin periodane; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene; benzene;
DOI:10.1016/j.ejmech.2012.01.014

Reference yield:

: 1370531-29-5
N-(4-methoxylphenyl)-4-methyl-3-nitro-1-benzenecarbothioamide

: 1370531-40-0
(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolyl[4-(6-methoxy-1,3-benzothiazol-2-yl)-2-nitrophenyl]methanone

Guidance literature:: Multi-step reaction with 4 steps

1: Dess-Martin periodane / dichloromethane / 20 °C

2: pyridine; tetra-n-butylammonium permanganate / 12 h / 20 °C

3: thionyl chloride; N,N-dimethyl-formamide / benzene / Reflux

4: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

With pyridine; thionyl chloride; tetra-n-butylammonium permanganate; Dess-Martin periodane; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1016/j.ejmech.2012.01.014