(5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

Base Information

Chemical Name:(5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one
CAS No.:1010833-16-5
Molecular Formula:C₁₁H₈Cl₂N₂OS
Molecular Weight:287.169
Hs Code.:

Synonyms:(5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

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Technology Process of (5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

There total 5 articles about (5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₁H₉Cl₂BrO₂

: 17356-08-0
thiourea

: 1010833-16-5
(5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

Guidance literature:: C₁₁H₉Cl₂BrO₂; thiourea; In water; acetone; at 25 ℃; for 1h;

With sodium hydrogencarbonate; In water; Further stages.;
DOI:10.1016/j.tetlet.2007.12.029

Reference yield:

: BrH*C₁₂H₁₂Cl₂N₂O₂S

: 1010833-16-5
(5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.3998/ark.5550190.0011.b24

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 1010833-16-5
(5Z)-2-amino-[5-(2,4-dichlorobenzylidene)]-5,6-dihydro-1,3-thiazin-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1,4-diaza-bicyclo[2.2.2]octane

2: lithium bromide / acetonitrile / 20 °C / Acidic conditions

3: acetone; water / 20 °C

4: sodium hydrogencarbonate / water

With 1,4-diaza-bicyclo[2.2.2]octane; sodium hydrogencarbonate; lithium bromide; In water; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2013.10.017