3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

Base Information

Chemical Name:3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose
CAS No.:134428-55-0
Molecular Formula:C₁₆H₁₉NO₅
Molecular Weight:305.331
Hs Code.:

Synonyms:3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

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Chemical Property of 3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

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Technology Process of 3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

There total 6 articles about 3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3-benzamido-3,6-dideoxy-D-arabino-hexofuranos-5-ulose

: 67-64-1
acetone

: 134428-55-0
3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

Guidance literature:: With toluene-4-sulfonic acid; copper(II) sulfate; Ambient temperature;
DOI:10.1016/0008-6215(91)84152-5

Reference yield:

: 134428-53-8
methyl 3-benzamido-3,6-dideoxy-α-D-arabino-hex-5-enopyranoside

: 134428-55-0
3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Amberlyst 15 (H+) resin / dimethylformamide; H₂O / 5 h

2: 92 percent / CuSO₄, p-toluenesulfonic acid / Ambient temperature

With Amberlyst 15 (H+) resin; toluene-4-sulfonic acid; copper(II) sulfate; In water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)84152-5

Reference yield:

: 134428-52-7
methyl 3-azido-4-O-benzoyl-3,6-dideoxy-α-D-arabino-hex-5-enopyranoside

: 134428-55-0
3-benzamido-3,6-dideoxy-1,2-O-isopropylidene-β-D-arabino-hexofuranos-5-ulose

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / NaBH₄, Te / ethanol / Ambient temperature

2: 95 percent / Amberlyst 15 (H+) resin / dimethylformamide; H₂O / 5 h

3: 92 percent / CuSO₄, p-toluenesulfonic acid / Ambient temperature

With tellurium; sodium tetrahydroborate; Amberlyst 15 (H+) resin; toluene-4-sulfonic acid; copper(II) sulfate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)84152-5