Iminostilbene

Base Information

Chemical Name:Iminostilbene
CAS No.:256-96-2
Molecular Formula:C14H11N
Molecular Weight:193.248
Hs Code.:29339900
European Community (EC) Number:205-970-0
NSC Number:123458
UNII:J411KQJ8C2
DSSTox Substance ID:DTXSID90871625
Nikkaji Number:J24.602F
Wikipedia:Dibenzazepine
Wikidata:Q61388
Metabolomics Workbench ID:56798
ChEMBL ID:CHEMBL243596
Mol file:256-96-2.mol

Synonyms:dibenzazepine;GSI XX;iminostilbene;iminostilbene, 10-(13)C-labeled

Suppliers and Price of Iminostilbene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Iminostilbene
10g
$ 340.00

TCI Chemical
Iminostilbene >98.0%(GC)(N)
5g
$ 41.00

TCI Chemical
Iminostilbene >98.0%(GC)(N)
25g
$ 116.00

SynQuest Laboratories
Iminostilbene 97.0%
100 g
$ 88.00

SynQuest Laboratories
Iminostilbene 97.0%
25 g
$ 29.00

Sigma-Aldrich
Carbamazepine Related Compound B United States Pharmacopeia (USP) Reference Standard
50mg
$ 1260.00

Sigma-Aldrich
5H-Dibenz[b,f]azepine 97%
1g
$ 53.40

Sigma-Aldrich
5H-Dibenz[b,f]azepine 97%
5g
$ 58.00

Sigma-Aldrich
Iminostilbene: Carbamazepine Related Compound B Pharmaceutical Secondary Standard; Certified Reference Material
500mg
$ 88.80

Matrix Scientific
5H-Dibenzo[b,f]azepine >95%
25g
$ 41.00

Total 144 raw suppliers

Chemical Property of Iminostilbene

Chemical Property:

Appearance/Colour:Yellow to orange-yellow fine powder
Vapor Pressure:4.81E-05mmHg at 25°C
Melting Point:197-201 °C
Refractive Index:n20/D 1.523(lit.)
Boiling Point:349.1 °C at 760 mmHg
PKA:1.71±0.20(Predicted)
Flash Point:178.4 °C
PSA：12.03000
Density:1.116 g/cm³
LogP:4.05200
Storage Temp.:Refrigerator
Solubility.:dioxane: 50 mg/mL, clear
Water Solubility.:Soluble in ethyl acetate (25 mg/ml), water (partly), dioxane, chloroform, and DMSO.
XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:193.089149355
Heavy Atom Count:15
Complexity:222

Purity/Quality:

99%, ^*data from raw suppliers

Iminostilbene ^*data from reagent suppliers

Safty Information:

Pictogram(s): C,Xi,N,Xn
Hazard Codes:C,Xi,N,Xn
Statements: 34-51/53-22-36/37/38
Safety Statements: 26-36/37/39-45-61-27-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=CC=CC=C3N2
Uses Iminostilbene is mainly used as a pharmaceutical intermediate for the production of carbamazepine, Oxcarbazepine, and rhodium catalyst ligand. It is a metabolite of of carbamazepine which is used primarily in the treatment of epilepsy and neuropathic pain.

Technology Process of Iminostilbene

There total 52 articles about Iminostilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 19209-60-0
N-acetyl iminostilbene

: 256-96-2
dibenzoazepine

Guidance literature:: With triethyl borane; sodium hydroxide; In tert-butyl methyl ether; at 80 ℃; for 6h; Inert atmosphere; Sealed tube;

Reference yield: 99.0%

: 2039-88-5
2-bromostyrene

: 95-51-2
o-chloroaniline

: 256-96-2
dibenzoazepine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; DavePhos; In 1,4-dioxane; at 110 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ja107511g