C₁₄H₁₈BrNO₄

Base Information

Chemical Name:C₁₄H₁₈BrNO₄
CAS No.:1534328-69-2
Molecular Formula:C₁₄H₁₈BrNO₄
Molecular Weight:344.205
Hs Code.:

C<sub>14</sub>H<sub>18</sub>BrNO<sub>4</sub>

Synonyms:C₁₄H₁₈BrNO₄

Suppliers and Price of C₁₄H₁₈BrNO₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₈BrNO₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₈BrNO₄

There total 1 articles about C₁₄H₁₈BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 6940-50-7
4-bromo-DL-mandelic acid

: 27532-96-3
glycine tert-butyl ester hydrochloride

: 1534328-69-2
C₁₄H₁₈BrNO₄

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja411547j

Reference yield: 83.0%

: 1534328-69-2
C₁₄H₁₈BrNO₄

: 7693-46-1
4-Nitrophenyl chloroformate

: 1534328-70-5
C₂₁H₂₁BrN₂O₈

Guidance literature:: With pyridine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja411547j

Reference yield:

: 1534328-69-2
C₁₄H₁₈BrNO₄

: C₂₁H₃₀BN₃O₇

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / dichloromethane; 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

With pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/ja411547j