zinc-5,15,20-tris(3,5-di-tert-butylphenyl)-10-(4-hydroxyphenyl)porphyrin

Base Information

• Chemical Name: zinc-5,15,20-tris(3,5-di-tert-butylphenyl)-10-(4-hydroxyphenyl)porphyrin
• CAS No.: 886359-71-3
• Molecular Formula: C₆₈H₇₆N₄OZn
• Molecular Weight: 1030.77

Synonyms:zinc-5,15,20-tris(3,5-di-tert-butylphenyl)-10-(4-hydroxyphenyl)porphyrin

Chemical Property of zinc-5,15,20-tris(3,5-di-tert-butylphenyl)-10-(4-hydroxyphenyl)porphyrin

Chemical Property:

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Technology Process of zinc-5,15,20-tris(3,5-di-tert-butylphenyl)-10-(4-hydroxyphenyl)porphyrin

There total 2 articles about zinc-5,15,20-tris(3,5-di-tert-butylphenyl)-10-(4-hydroxyphenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-(10,15,20-tris-(3,5-di-tert-butylphenyl)porphyrin-5-yl)phenol → 5,10,15-tris(3,5-di-tetr-butylphenyl)-20-(4-hydroxyphenyl)porphyrinato zinc(II) (886359-71-3)

Guidance literature:

With zinc diacetate; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1016/j.tetlet.2010.02.137

Reference yield: 70.0%

zinc(II) acetate dihydrate (5970-45-6) + 10-(4-hydroxyphenyl)-5,15,20-tris{(3,5-di-tert-butyl)phenyl}porphyrin → 5,10,15-tris(3,5-di-tetr-butylphenyl)-20-(4-hydroxyphenyl)porphyrinato zinc(II) (886359-71-3)

Guidance literature:

In tetrahydrofuran; methanol; for 1.5h; Reflux;

Reference yield: 87.0%

5,10,15-tris(3,5-di-tetr-butylphenyl)-20-(4-hydroxyphenyl)porphyrinato zinc(II) (886359-71-3) + 1,10-dibromodecane (4101-68-2) → C78H95BrN4OZn

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 13h;

DOI:10.1002/asia.201901711

upstream raw materials:

zinc(II) acetate dihydrate

Downstream raw materials:

C₈₈H₉₉BN₄O₄Zn

C₁₁₀H₁₀₈ClCuN₁₀OSZn

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