C₂₃H₃₂O₆

Base Information

• Chemical Name: C₂₃H₃₂O₆
• CAS No.: 1123212-95-2
• Molecular Formula: C₂₃H₃₂O₆
• Molecular Weight: 404.503
• Mol file: 1123212-95-2.mol

Synonyms:C₂₃H₃₂O₆

Chemical Property of C₂₃H₃₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₂O₆

There total 2 articles about C₂₃H₃₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

benzyl bromide (100-39-0) + 3-C-(3-butenyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose (156311-59-0) → C23H32O6 (1123212-95-2)

Guidance literature:

With sodium hydride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 0 ℃; for 4h;

DOI:10.1016/j.tetlet.2011.09.104

Reference yield:

1,2:5,6-di-O-isopropylidene-α-D-hexofuran-3-ulose (2847-00-9) → C23H32O6 (1123212-95-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: magnesium / diethyl ether

1.2: 2 h / 0 °C

2.1: sodium hydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 4 h / 0 °C

With sodium hydride; magnesium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;

DOI:10.1016/j.tetlet.2011.09.104

Reference yield: 80.0%

C23H32O6 (1123212-95-2) → C22H30O7

Guidance literature:

With sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; water; at 0 ℃; for 12h;

DOI:10.1016/j.tetlet.2011.09.104

upstream raw materials:

benzyl bromide

3-C-(3-butenyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

1,2:5,6-di-O-isopropylidene-α-D-hexofuran-3-ulose

Downstream raw materials:

C₂₃H₂₈O₅

C₂₄H₃₀O₅