(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

Base Information

Chemical Name:(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol
CAS No.:881831-93-2
Molecular Formula:C₁₉H₃₀O
Molecular Weight:274.447
Hs Code.:

Synonyms:(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

Chemical Property:

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Technology Process of (2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

There total 3 articles about (2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51318-62-8,51371-55-2,26918-14-9
ethyl 4-bromo-3-methylcrotonate

: 881831-93-2
(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc; copper diacetate; acetic acid / 1,4-dioxane / 8 h / Reflux

1.2: Reformatsky Reaction / 0.25 h

2.1: lithium aluminium tetrahydride / diethyl ether / 1 h / -78 - 0 °C

With lithium aluminium tetrahydride; copper diacetate; acetic acid; zinc; In 1,4-dioxane; diethyl ether; 1.1: |Reformatsky Reaction;
DOI:10.1021/acs.jmedchem.5b00829

Reference yield:

: 881831-85-2
(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

: 881831-93-2
(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -78 - 0 ℃; for 1h;
DOI:10.1021/acs.jmedchem.5b00829

Reference yield:

: 638-10-8
ethyl 3-methylbut-2-enoate

: 881831-93-2
(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 6 h / Reflux

2.1: zinc; copper diacetate; acetic acid / 1,4-dioxane / 8 h / Reflux

2.2: Reformatsky Reaction / 0.25 h

3.1: lithium aluminium tetrahydride / diethyl ether / 1 h / -78 - 0 °C

With N-Bromosuccinimide; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); copper diacetate; acetic acid; zinc; In 1,4-dioxane; tetrachloromethane; diethyl ether; 2.1: |Reformatsky Reaction;
DOI:10.1021/acs.jmedchem.5b00829