(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

Base Information

Chemical Name:(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid
CAS No.:881831-85-2
Molecular Formula:C₁₉H₂₈O₂
Molecular Weight:288.43
Hs Code.:

Synonyms:(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

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Chemical Property of (2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

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Technology Process of (2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

There total 2 articles about (2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(3-methyl) butyl-3-cyclopropyl-2-cyclohexenone

: 51318-62-8,51371-55-2,26918-14-9
ethyl 4-bromo-3-methylcrotonate

: 881831-85-2
(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

Guidance literature:: 2-(3-methyl) butyl-3-cyclopropyl-2-cyclohexenone; ethyl 4-bromo-3-methylcrotonate; With copper diacetate; acetic acid; zinc; In 1,4-dioxane; for 8h; Reflux;

With hydrogenchloride; In 1,4-dioxane; water; for 0.25h;
DOI:10.1021/acs.jmedchem.5b00829

Reference yield:

: 638-10-8
ethyl 3-methylbut-2-enoate

: 881831-85-2
(2Z)-4-(2′-(3-methyl)butyl-3′-cyclopropyl-2′-cyclohexen-1′-ylidene)-3-methyl-2-butenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 6 h / Reflux

2.1: zinc; copper diacetate; acetic acid / 1,4-dioxane / 8 h / Reflux

2.2: Reformatsky Reaction / 0.25 h

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); copper diacetate; acetic acid; zinc; In 1,4-dioxane; tetrachloromethane; 2.1: |Reformatsky Reaction;
DOI:10.1021/acs.jmedchem.5b00829