ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate

Base Information

• Chemical Name: ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate
• CAS No.: 938447-19-9
• Molecular Formula: C₂₇H₃₃N₃O₈S₂
• Molecular Weight: 591.706

Synonyms:ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate

Chemical Property of ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate

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Technology Process of ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate

There total 1 articles about ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

3-[(E)-3-({1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)prop-1-enyl]benzonitrile (938447-12-2) + ethyl 2-(chlorosulfonyl)acetate (55896-93-0) → ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate (938447-19-9)

Guidance literature:

With triethylamine; In 1,2-dichloro-ethane; at 0 ℃; for 3h;

DOI:10.1016/j.bmc.2007.03.066

Reference yield: 91.0%

ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate (938447-19-9) → ethyl [(((E)-3-{3-[amino(imino)methyl]phenyl}prop-2-enyl){1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate hydrochloride

Guidance literature:

ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate; With hydrogenchloride; In ethanol; chloroform; at 5 ℃; for 22h;

With ammonium acetate; In ethanol; at 20 ℃; for 24h; Further stages.;

DOI:10.1016/j.bmc.2007.03.066

Reference yield: 76.0%

ethyl [([(E)-3-(3-cyanophenyl)prop-2-enyl]{1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)sulfonyl]acetate (938447-19-9) → ethyl {[((E)-3-{3-[(amino)(hydroxyimino)methyl]phenyl}prop-2-enyl){1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino]sulfonyl}acetate

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; at 80 ℃; for 14h;

DOI:10.1016/j.bmc.2007.03.066

upstream raw materials:

3-[(E)-3-({1-[(2,5-dimethoxyphenyl)sulfonyl]piperidin-4-yl}amino)prop-1-enyl]benzonitrile

ethyl 2-(chlorosulfonyl)acetate

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