1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

Base Information

Chemical Name:1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol
CAS No.:104976-48-9
Molecular Formula:C₂₆H₃₆O₇
Molecular Weight:460.568
Hs Code.:

Synonyms:1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

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Chemical Property of 1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

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Technology Process of 1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

There total 3 articles about 1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 104976-47-8
1D-(1,2,4/3,5)-1-O-Acetyl-2,3-di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

: 104976-48-9
1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

Guidance literature:: With sodium methylate; In methanol; for 120h; Ambient temperature;

Reference yield:

: 104976-46-7
1D-(1,2,4/3,5)-1-O-Acetyl-2,3-di-O-benzyl-5-C-hydroxymethyl-4-O-methyl-1,2,3,4-cyclohexantetrol

: 104976-48-9
1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NEt(iPr)2 / CH₂Cl₂ / 20 h / Ambient temperature

2: 95 percent / NaOMe (1M) / methanol / 120 h / Ambient temperature

With sodium methylate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;

Reference yield:

: 104976-12-7
1D-(1,2,4/3,5)-1-O-Acetyl-2,3-di-O-benzyl-5-C-<(tert-butyldiphenylsilyloxy)methyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

: 104976-48-9
1D-(1,2,4/3,5)-2,3-Di-O-benzyl-5-C-<(2-methoxyethoxy)methoxymethyl>-4-O-methyl-1,2,3,4-cyclohexantetrol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / Bu₄NF*3H₂O / tetrahydrofuran / 6 h / Ambient temperature

2: 93 percent / NEt(iPr)2 / CH₂Cl₂ / 20 h / Ambient temperature

3: 95 percent / NaOMe (1M) / methanol / 120 h / Ambient temperature

With tetrabutyl ammonium fluoride; sodium methylate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane;