4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole

Base Information

• Chemical Name: 4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole
• CAS No.: 1160754-33-5
• Molecular Formula: C₃₄H₃₄N₄O₂
• Molecular Weight: 530.67

Synonyms:4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole

Chemical Property of 4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole

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Technology Process of 4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole

There total 1 articles about 4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,1'-bis(t-butoxycarbonyl)-4,4'-bis(2,6-dimethyl-4-methoxyphenyl)-6,6'-dimethyl-2,2'-bisbenzimidazole → 4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole (1160754-33-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1039/b820502g

Reference yield: 78.0%

4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole (1160754-33-5) + α,α'-dibromo-o-xylene (91-13-4) → 6,11-dihydro-1,16-bis(4-methoxyphenyl-2,6-dimethyl)-3,14-dimethylbisbenzimidazo[1,2-b:2',1'-d][2,5]benzodiazocine (1160754-35-7)

Guidance literature:

With caesium carbonate; sodium iodide; In tetrahydrofuran; at 60 ℃; for 168h; Inert atmosphere;

DOI:10.1039/b820502g

Reference yield: 71.0%

4,4'-bis(4-methoxyphenyl-2,6-dimethyl)-6,6'-dimethyl-2,2'-bibenzimidazole (1160754-33-5) + 1,3-dibromo-propane (109-64-8) → 7,8-dihydro-1,13-bis(4-methoxyphenyl-2,6-dimethyl)-3,11-dimethyl-6H-benzimidazo[2',1':3,4][1,4]diazepino[1,2-a]benzimidazole (1160754-37-9)

Guidance literature:

With caesium carbonate; sodium iodide; In tetrahydrofuran; at 70 ℃; for 120h; Inert atmosphere;

DOI:10.1039/b820502g

Downstream raw materials:

7,8-dihydro-1,13-bis(4-methoxyphenyl-2,6-dimethyl)-3,11-dimethyl-6H-benzimidazo[2',1':3,4][1,4]diazino[1,2-a]benz-imidazole

7,8-dihydro-1,13-bis(4-methoxyphenyl-2,6-dimethyl)-3,11-dimethyl-6H-benzimidazo[2',1':3,4][1,4]diazepino[1,2-a]benzimidazole

6,11-dihydro-1,16-bis(4-methoxyphenyl-2,6-dimethyl)-3,14-dimethylbisbenzimidazo[1,2-b:2',1'-d][2,5]benzodiazocine

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