C₁₂H₁₆BrN

Base Information

Chemical Name:C₁₂H₁₆BrN
CAS No.:1609646-98-1
Molecular Formula:C₁₂H₁₆BrN
Molecular Weight:254.17
Hs Code.:

Synonyms:C₁₂H₁₆BrN

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Chemical Property of C₁₂H₁₆BrN

Chemical Property:

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Technology Process of C₁₂H₁₆BrN

There total 4 articles about C₁₂H₁₆BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1609646-95-8
C₁₂H₁₆BrN

: 1609646-98-1
C₁₂H₁₆BrN

Guidance literature:: In acetonitrile; for 15h; Reflux;
DOI:10.1055/s-0033-1340250

Reference yield:

: 922-63-4
ethylacrolein

: 1609646-98-1
C₁₂H₁₆BrN

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / dichloromethane / 2.5 h / 0 - 20 °C

2: titanium tetrachloride; triethylamine / diethyl ether / 15 h / 0 - 20 °C

3: sodium tetrahydroborate / methanol / 20 °C

4: acetonitrile / 15 h / Reflux

With sodium tetrahydroborate; bromine; titanium tetrachloride; triethylamine; In methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1055/s-0033-1340250

Reference yield:

: C₁₂H₁₅Br₂N

: 1609646-98-1
C₁₂H₁₆BrN

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 20 °C

2: acetonitrile / 15 h / Reflux

With sodium tetrahydroborate; In methanol; acetonitrile;
DOI:10.1055/s-0033-1340250