(E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

Base Information

Chemical Name:(E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide
CAS No.:1355970-62-5
Molecular Formula:C₁₅H₁₅N₃O₆S
Molecular Weight:365.367
Hs Code.:

Synonyms:(E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

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Chemical Property of (E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

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Technology Process of (E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

There total 3 articles about (E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 4521-33-9
5-nitro-2-thiophenecarboxaldehyde

: 3291-03-0
3,4,5-trimethoxybenzohydrazide

: 1355970-62-5
(E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

Guidance literature:: In ethanol; for 1h; Reflux;
DOI:10.13005/ojc/330126

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 1355970-62-5
(E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 20 °C / Reflux

2: methanol / 2 h / Reflux

With hydrazine hydrate; In methanol;
DOI:10.1016/j.ejmech.2015.02.041

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 1355970-62-5
(E)-3,4,5-trimethoxy-N'-((5-nitrothiophen-2-yl)methylene)benzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone / 12 h / Reflux

2: hydrazine hydrate / methanol / 20 °C / Reflux

3: methanol / 2 h / Reflux

With tetra-(n-butyl)ammonium iodide; potassium carbonate; hydrazine hydrate; In methanol; acetone;
DOI:10.1016/j.ejmech.2015.02.041