3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

Base Information

Chemical Name:3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride
CAS No.:1590687-32-3
Molecular Formula:C₁₃H₁₁N₄O₂*Cl
Molecular Weight:290.709
Hs Code.:

Synonyms:3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

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Technology Process of 3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

There total 1 articles about 3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7164-98-9
1-phenylimidazole

: 4270-27-3
6-chlorouracil

: 1590687-32-3
3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

Guidance literature:: In chlorobenzene; for 8h; Reflux;
DOI:10.1039/c3ob42462f

Reference yield: 80.0%

: 1590687-32-3
3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

: C₁₃H₁₀N₄O₂

Guidance literature:: With Amberlite IRA-400 (OH^-form) resin; In water;
DOI:10.1039/c3ob42462f

Reference yield:

: 1590687-32-3
3-(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-4-yl)-1-phenyl-1H-imidazolium chloride

: 6,8-dioxo-1,10,10-triphenyl-6,7,8,10-tetrahydro-1H-imidazo-[2′,1′:3,4][1,4,2]diazaborolo[1,5-c]pyrimidinium-10-ide

Guidance literature:: Multi-step reaction with 2 steps

1: Amberlite IRA-400 (OH^-form) resin / water

2: 1,4-dioxane; dichloromethane / 24 h / 200 °C / Inert atmosphere; Schlenk technique

With Amberlite IRA-400 (OH^-form) resin; In 1,4-dioxane; dichloromethane; water;
DOI:10.1039/c3ob42462f