2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

Base Information

Chemical Name:2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid
CAS No.:1055303-47-3
Molecular Formula:C₂₆H₂₄O₆S
Molecular Weight:464.539
Hs Code.:

Synonyms:2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

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Chemical Property of 2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

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Technology Process of 2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

There total 3 articles about 2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: C₂₈H₂₅Cl₃O₆S

: 1055303-47-3
2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

Guidance literature:: With acetic acid; zinc; In dichloromethane; for 48h;

Reference yield:

: 1055304-08-9
2,2,2-trichloroethyl 2-(bromomethyl)benzoate

: 1055303-47-3
2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

3: acetic acid; zinc / dichloromethane / 48 h

With dmap; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 7115-89-1
2-(bromomethyl)benzoic acid

: 1055303-47-3
2-[3-(1-methoxycarbonyl-2-phenyl-ethoxycarbonylmethyl)-phenylsulfanylmethyl]-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4: acetic acid; zinc / dichloromethane / 48 h

With dmap; caesium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; zinc; In dichloromethane; N,N-dimethyl-formamide;