5-(hexyloxy)-2-nitrophenol

Base Information

• Chemical Name: 5-(hexyloxy)-2-nitrophenol
• CAS No.: 885620-28-0
• Molecular Formula: C₁₂H₁₇NO₄
• Molecular Weight: 239.271
• Mol file: 885620-28-0.mol

Synonyms:5-(hexyloxy)-2-nitrophenol

Chemical Property of 5-(hexyloxy)-2-nitrophenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 5-(hexyloxy)-2-nitrophenol

There total 3 articles about 5-(hexyloxy)-2-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

n-hexyl resorcinol (67089-07-0) → 5-(hexyloxy)-2-nitrophenol (885620-28-0)

Guidance literature:

With hydrogenchloride; sodium nitrate; acetic anhydride; In diethyl ether; dichloromethane; water; at 20 ℃; for 4h;

DOI:10.1002/hlca.200690035

Reference yield:

1-bromo-hexane (111-25-1) → 5-(hexyloxy)-2-nitrophenol (885620-28-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / NaNO₃; HCl; Ac₂O / CH₂Cl₂; diethyl ether; H₂O / 4 h / 20 °C

With hydrogenchloride; sodium nitrate; acetic anhydride; In diethyl ether; dichloromethane; water; 1: Williamson reaction;

DOI:10.1002/hlca.200690035

Reference yield:

recorcinol (108-46-3) → 5-(hexyloxy)-2-nitrophenol (885620-28-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / NaNO₃; HCl; Ac₂O / CH₂Cl₂; diethyl ether; H₂O / 4 h / 20 °C

With hydrogenchloride; sodium nitrate; acetic anhydride; In diethyl ether; dichloromethane; water; 1: Williamson reaction;

DOI:10.1002/hlca.200690035

upstream raw materials:

n-hexyl resorcinol

1-bromo-hexane

recorcinol