1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

Base Information

Chemical Name:1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)
CAS No.:138149-64-1
Molecular Formula:C₃₆H₄₈N₄O₈P₄
Molecular Weight:788.694
Hs Code.:

Synonyms:1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

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Chemical Property of 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

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Technology Process of 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

There total 5 articles about 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 138999-82-3
tetramethyl 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetra(phenylphosphinate)

: 138149-64-1
1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

Guidance literature:: With hydrogenchloride; for 16h; Heating;
DOI:10.1055/s-1992-34177

Reference yield:

: 2946-61-4
phenylphosphonous acid dimethyl ester

: 138149-64-1
1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / molecular sieves (3 A) / tetrahydrofuran / 16 h / Heating

2: 88 percent / 6M HCl / 16 h / Heating

With hydrogenchloride; 3 A molecular sieve; In tetrahydrofuran;
DOI:10.1055/s-1992-34177

Reference yield:

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 138149-64-1
1,4,7,10-tetraazacyclododecane-1,4,7,10-tetrayltetramethylenetetrakis(phenylphosphinic acid)

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / molecular sieves (3 A) / tetrahydrofuran / 16 h / Heating

2: 88 percent / 6M HCl / 16 h / Heating

With hydrogenchloride; 3 A molecular sieve; In tetrahydrofuran;
DOI:10.1055/s-1992-34177