benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

Base Information

Chemical Name:benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate
CAS No.:1000872-32-1
Molecular Formula:C₃₀H₃₆ClFN₂O₈S
Molecular Weight:639.142
Hs Code.:

Synonyms:benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

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Chemical Property of benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

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Technology Process of benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

There total 3 articles about benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 243983-70-2,243984-10-3
ethyl (6RS)-6-[N-(2-chloro-4-fluorophenyl)sulfamoyl]cyclohex-1-ene-1-carboxylate

: 1000872-61-6
benzyl N-[(iodomethoxy)carbonyl]-D-leucinate

: 1000872-32-1
benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 2.5h;

Reference yield:

: 1000872-49-0
benzyl N-[(chloromethoxy)carbonyl]-D-leucinate

: 1000872-32-1
benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetonitrile / 1.5 h / 60 °C

2: potassium carbonate / acetonitrile / 2.5 h / 20 °C

With potassium carbonate; sodium iodide; In acetonitrile;

Reference yield:

: 17664-93-6
(R)-benzyl 2-amino-4-methylpentanoate p-toluenesulfonate salt

: 1000872-32-1
benzyl N-{[((2-chloro-4-fluorophenyl){[2-(ethoxycarbonyl)cyclohex-2-en-1-yl]sulfonyl}amino)methoxy]carbonyl}-D-leucinate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / diethyl ether / 5.67 h / 0 °C

2: sodium iodide / acetonitrile / 1.5 h / 60 °C

3: potassium carbonate / acetonitrile / 2.5 h / 20 °C

With pyridine; potassium carbonate; sodium iodide; In diethyl ether; acetonitrile;