C₅₂H₃₉B₂F₄N₅O₃

Base Information

Chemical Name:C₅₂H₃₉B₂F₄N₅O₃
CAS No.:1379764-33-6
Molecular Formula:C₅₂H₃₉B₂F₄N₅O₃
Molecular Weight:879.529
Hs Code.:

C<sub>52</sub>H<sub>39</sub>B<sub>2</sub>F<sub>4</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₅₂H₃₉B₂F₄N₅O₃

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Chemical Property of C₅₂H₃₉B₂F₄N₅O₃

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Technology Process of C₅₂H₃₉B₂F₄N₅O₃

There total 7 articles about C₅₂H₃₉B₂F₄N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.5%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1379764-36-9
C₄₀H₂₆BF₂N₃O₄

: 1379764-33-6
C₅₂H₃₉B₂F₄N₅O₃

Guidance literature:: 2,4-dimethyl-1H-pyrrole; C₄₀H₂₆BF₂N₃O₄; With trifluoroacetic acid; In dichloromethane; for 3h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 1h; Inert atmosphere;

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1h; Inert atmosphere;
DOI:10.1039/c3cc40471d

Reference yield:

: 1195110-34-9
4,4'-(5,5-difluoro-1,9-diphenyl-5H-4l4,5l4-dipyrrolo[1,2-c:2',1'-f][1,3,5,2]triazaborinine-3,7-diyl)diphenol

: 1379764-33-6
C₅₂H₃₉B₂F₄N₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 0 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 3 h / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere

With boron trifluoride diethyl etherate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103074

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1379764-33-6
C₅₂H₃₉B₂F₄N₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 0 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 3 h / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere

With boron trifluoride diethyl etherate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201103074