4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

Base Information

Chemical Name:4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine
CAS No.:1197982-32-3
Molecular Formula:C₃₀H₃₄N₁₂O₈
Molecular Weight:690.676
Hs Code.:

Synonyms:4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

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Chemical Property of 4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

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Technology Process of 4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

There total 1 articles about 4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1197981-97-7
p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

: 499195-32-3
1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

: 1197982-32-3
4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

Guidance literature:: p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside; 1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine; With N-iodo-succinimide; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -40 - -20 ℃; Inert atmosphere;
DOI:10.1039/b907518f