p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

Base Information

Chemical Name:p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside
CAS No.:1197981-97-7
Molecular Formula:C₁₇H₂₀N₆O₅S
Molecular Weight:420.449
Hs Code.:

Synonyms:p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

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Technology Process of p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

There total 1 articles about p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₆N₆O₃S

: 108-24-7
acetic anhydride

: 1197981-97-7
p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

Guidance literature:: With pyridine; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b907518f

Reference yield: 84.0%

: 1197981-97-7
p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside

: 499195-32-3
1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

: 1197982-32-3
4-O-(2',6'-di-azido-2',6'-dideoxy-3',4'-di-O-acetyl-α-D-mannopyranosyl)-1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine

Guidance literature:: p-methylphenyl 2,6-di-azido-3,4-di-O-acetyl-1-thio-2,6-di-deoxy-α-D-mannopyranoside; 1,3-di-azido-5,6-di-O-benzyl-2-deoxystreptamine; With N-iodo-succinimide; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In diethyl ether; dichloromethane; at -40 - -20 ℃; Inert atmosphere;
DOI:10.1039/b907518f