6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

Base Information

Chemical Name:6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone
CAS No.:97855-74-8
Molecular Formula:C₂₀H₃₂O₃
Molecular Weight:320.472
Hs Code.:

Synonyms:6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

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Chemical Property of 6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

Chemical Property:

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Technology Process of 6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

There total 19 articles about 6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97868-04-7
(2R,4aS,8aS)-(-)-1,2,3,4,4a,5,6,7,8,8a-decahydro-2α-hydroxy-5,5,8aβ-trimethyl-1-oxonaphthalene

: 97855-74-8
6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 11 steps

1: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

2: NaBH₄ / methanol / 0.33 h / Ambient temperature

3: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

4: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

5: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

6: 88 percent / Florisil, PCC / CH₂Cl₂ / 1 h / Ambient temperature

7: 98 percent / toluene-p-sulphonic acid / benzene / 0.33 h / Heating

8: 1. osmium tetraoxide; 2.) sodium periodate / 1.) diethyl ether, water, rt, 5 min; 2.) rt, 10 h.

9: 1.) lithium diisopropylamide (LDA) / 1.) THF, -78 deg C; 2.) THF, rt, 1 h.

10: 98 percent / H₂ / 10 percent palladium-charcoal / ethanol

With lead(IV) acetate; sodium hydroxide; sodium tetrahydroborate; florisil; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; benzene;

Reference yield:

: 97855-67-9
(-)-(2R,4aS,8aS)-2-bromo-3,4,4a,5,6,7,8,8a-octahydro-5,5,8a-trimethylnaphthalen-1(2H)-one

: 97855-74-8
6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 12 steps

1: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

2: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

3: NaBH₄ / methanol / 0.33 h / Ambient temperature

4: 98 percent / tributylphosphine / tetrahydrofuran / 0.33 h / Ambient temperature

5: 91 percent / hydrogen peroxide / tetrahydrofuran / 10 h / Ambient temperature

6: 1.) lithium aluminium hydride; 2.) sodium hydroxide / 1.) diethyl ether, rt, 30 min; 2.) water, 30 min.

7: 88 percent / Florisil, PCC / CH₂Cl₂ / 1 h / Ambient temperature

8: 98 percent / toluene-p-sulphonic acid / benzene / 0.33 h / Heating

9: 1. osmium tetraoxide; 2.) sodium periodate / 1.) diethyl ether, water, rt, 5 min; 2.) rt, 10 h.

10: 1.) lithium diisopropylamide (LDA) / 1.) THF, -78 deg C; 2.) THF, rt, 1 h.

11: 98 percent / H₂ / 10 percent palladium-charcoal / ethanol

With lead(IV) acetate; sodium hydroxide; sodium tetrahydroborate; florisil; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; tributylphosphine; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 97855-74-8
6-[2-((1S,2S)-2-[1,3]Dioxolan-2-yl-2,6,6-trimethyl-cyclohexyl)-ethyl]-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium diisopropylamide (LDA) / 1.) THF, -78 deg C; 2.) THF, rt, 1 h.

2: 98 percent / H₂ / 10 percent palladium-charcoal / ethanol

With hydrogen; lithium diisopropyl amide; palladium on activated charcoal; In ethanol;