C₃₃H₂₄IN₃O₆

Base Information

Chemical Name:C₃₃H₂₄IN₃O₆
CAS No.:1445712-19-5
Molecular Formula:C₃₃H₂₄IN₃O₆
Molecular Weight:685.475
Hs Code.:

C<sub>33</sub>H<sub>24</sub>IN<sub>3</sub>O<sub>6</sub>

Synonyms:C₃₃H₂₄IN₃O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₂₄IN₃O₆

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Technology Process of C₃₃H₂₄IN₃O₆

There total 5 articles about C₃₃H₂₄IN₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 609-67-6
2-Iodobenzoyl chloride

: 1445712-12-8
C₂₆H₂₁N₃O₅

: 1445712-19-5
C₃₃H₂₄IN₃O₆

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; Reflux;
DOI:10.1021/jf4011033

Reference yield:

: 105608-71-7
3',4'-didemethoxy-4-deoxy-3',4'-dihydro-3',4'-dioxopodophyllotoxin

: 1445712-19-5
C₃₃H₂₄IN₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1: chloroform / 5 h / 20 °C

2: tin(II) chloride dihdyrate / ethyl acetate / 7 h / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 0 °C / Reflux

With tin(II) chloride dihdyrate; triethylamine; In dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jf4011033

Reference yield:

: 518-28-5
podofilox

: 1445712-19-5
C₃₃H₂₄IN₃O₆

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen; palladium 10% on activated carbon; acetic acid / 5 h / 95 °C / 1520.1 Torr

2: nitric acid; propionic acid / 0.07 h / 0 °C

3: chloroform / 5 h / 20 °C

4: tin(II) chloride dihdyrate / ethyl acetate / 7 h / Inert atmosphere; Reflux

5: triethylamine / dichloromethane / 0 °C / Reflux

With tin(II) chloride dihdyrate; palladium 10% on activated carbon; hydrogen; nitric acid; acetic acid; propionic acid; triethylamine; In dichloromethane; chloroform; ethyl acetate;
DOI:10.1021/jf4011033