methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

Base Information

Chemical Name:methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester
CAS No.:1200406-24-1
Molecular Formula:C₄₄H₇₂NO₁₃PS
Molecular Weight:886.094
Hs Code.:

methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

Synonyms:methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

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Chemical Property of methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

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Technology Process of methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

There total 1 articles about methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200406-23-0
carbonic acid [2-[tert-butoxycarbonyl[6-(4-phenylbutoxy)hexyl]amino]-1-[4-(di-tert-butoxyphosphoryloxy)-3-hydroxymethylphenyl]ethyI]ester tert-butyl ester

: 124-63-0
methanesulfonyl chloride

: 1200406-24-1
methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

Guidance literature:: With 1,2,2,6,6-pentamethylpiperidine; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 1200406-24-1
methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

: 1200406-33-2
4-diethylaminoacetic acid [[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]] ester

: 1200406-81-0
[5-[1-(R)-hydroxy-2-[6-(4-phenylbutoxy)hexylamino]ethyl]-2-phosphonooxybenzyl]-(diethyl)-[[[11β,16α]-[16,17-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-oxy]-carbonylmethyl]ammonium chloride

Guidance literature:: methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester; With sodium iodide; In acetonitrile; at 20 ℃; for 1h;

4-diethylaminoacetic acid [[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]] ester; With silver trifluoromethanesulfonate; In dichloromethane; acetonitrile; at 20 ℃; Darkness;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃;

Reference yield:

: 1200406-24-1
methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester

: 1200406-42-3
4-methylpiperazinecarboxylic acid [[11β,16α]-[[((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]]ester

: 1308338-82-0
C₇₃H₁₀₉N₃O₁₇P⁽¹⁺⁾

Guidance literature:: methanesulfonic acid 5-[1-tert-butoxycarbonyloxy-2-[tert-butoxycarbonyl-[6-(4-phenylbutoxy)hexyl]amino]ethyl]-2-(di-tert-butoxyphosphoryloxy)benzyl ester; With sodium iodide; In acetonitrile; at 20 ℃; for 0.0833333h;

4-methylpiperazinecarboxylic acid [[11β,16α]-[[((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]]ester; In acetonitrile; at 20 ℃; for 24h;