5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

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Chemical Name:5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester
CAS No.:1041857-84-4
Molecular Formula:C₂₇H₃₂O₄SSi
Molecular Weight:480.7
Hs Code.:

Synonyms:5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

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Chemical Property of 5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

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Technology Process of 5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

There total 1 articles about 5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 13154-24-0
triisopropylsilyl chloride

: 1041857-83-3
5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid

: 1041857-84-4
5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2008.04.009

Reference yield: 40.0%

: 1041857-84-4
5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

: 84751-19-9
1-trimethylsilyl-4-t-butyl-1,3-butadiyne

: 1041857-85-5
5-(1-hydroxy-6,6-dimethyl-hepta-2,4-diynyl)-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester

Guidance literature:: 1-trimethylsilyl-4-t-butyl-1,3-butadiyne; With methyllithium; In diethyl ether; for 3h; Heating;

5-formyl-4-[4-(2-(methoxymethyl)-phenyl)-buta-1,3-diynyl]-thiophene-2-carboxylic acid triisopropylsilyl ester; In diethyl ether; at -72 - -48 ℃; for 2h; Further stages.;
DOI:10.1016/j.bmc.2008.04.009