CID 11228761

Base Information

• Chemical Name: CID 11228761
• CAS No.: 7335-65-1
• Molecular Formula: C2H4O2^.H4N2
• Molecular Weight: 92.0977
• Hs Code.: 29280000
• Mol file: 7335-65-1.mol

Synonyms:

Chemical Property of CID 11228761

Chemical Property:

• Appearance/Colour: white to light yellow
• Vapor Pressure: 10.2mmHg at 25°C
• Melting Point: 100-102 °C
• Refractive Index: 1.434
• Boiling Point: 117.1 °C at 760 mmHg
• Flash Point: 40 °C
• PSA: 89.34000
• Density: 1.161g/cm³
• LogP: 0.31030
• Storage Temp.: 0-6°C
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 92.058577502
• Heavy Atom Count: 6
• Complexity: 25.5

Purity/Quality:

99.0% ^*data from raw suppliers

Hydrazine acetate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): NT
• Hazard Codes: N-T,N,T
• Statements: 50/53-45-43-23/24/25-34-46
• Safety Statements: 61-60-53-45-36/37/39-28-27-26-23

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)[O-].[NH3+]N
• Uses: suzuki reaction Hydrazine acetate has been used in preparation of:2,3,5-tri-O-acetyl-α-L-arabinofuranosyl trichloroacetimidatedisaccharide 4-methoxyphenyl glycoside

Technology Process of CID 11228761

There total 3 articles about CID 11228761 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.5%

acetic acid (64-19-7,77671-22-8) → hydrazinium monoacetate (7335-65-1,13255-48-6)

Guidance literature:

With hydrazine hydrate; at 0 - 20 ℃; for 0.666667h;

Reference yield:

hydrazinium hydroxide + acetic acid (64-19-7,77671-22-8) → hydrazinium monoacetate (7335-65-1,13255-48-6)

Guidance literature:

In ethanol; evapn. in vac.; abs. alc.;

Reference yield:

hydrazin sulfate + barium(II) acetate (543-80-6) → hydrazinium monoacetate (7335-65-1,13255-48-6)

Guidance literature:

upstream raw materials:

acetic acid

barium(II) acetate

Downstream raw materials:

(3-methyl-2,4,6-trinitro-phenyl)-hydrazine

mesityl-glyoxal-2-hydrazone

acetic acid hydrazide

(2,4-dinitro-phenyl)-hydrazine

Refernces

• 1、 -. "A red ycin A derivatives, its preparation method, intermediate and application". Paragraph 0101; 0102. . Retrieved 2016/10/10.
• 2、 -. "TYROSINE KINASE INHIBITORS". Page/Page column 146-147. . Retrieved 2011/08/03.