2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

Base Information

Chemical Name:2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol
CAS No.:156422-24-1
Molecular Formula:C₂₆H₂₃ClO₃P₂
Molecular Weight:480.867
Hs Code.:

Synonyms:2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

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Chemical Property of 2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

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Technology Process of 2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

There total 4 articles about 2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 156422-15-0
Chloromethyl-phenyl-phosphinic acid 2-(diphenyl-phosphinoylmethyl)-phenyl ester

: 156422-24-1
2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; at -50 - 20 ℃;
DOI:10.1039/c39940000973

Reference yield:

: 70127-50-3
diphenyl(2-hydroxyphenylmethyl)phosphine oxide

: 156422-24-1
2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

Guidance literature:: Multi-step reaction with 2 steps

1: NEt₃ / benzene / 1 h / from RT to reflux

2: 25 percent / LiN(SiMe₃)2 / diethyl ether; tetrahydrofuran / -50 - 20 °C

With triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1039/c39940000973

Reference yield:

: 18544-92-8
1-Trimethylsilanyloxy-2-trimethylsilanyloxymethyl-benzene

: 156422-24-1
2-[(Chloromethyl-phenyl-phosphinoyl)-(diphenyl-phosphinoyl)-methyl]-phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 160 deg C, 2 h, 2.) EtOH, benzene, RT, 24 h

2: NEt₃ / benzene / 1 h / from RT to reflux

3: 25 percent / LiN(SiMe₃)2 / diethyl ether; tetrahydrofuran / -50 - 20 °C

With triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1039/c39940000973