Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

Base Information

Chemical Name:Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate
CAS No.:1242457-13-1
Molecular Formula:C₃₁H₃₉N₃O₅
Molecular Weight:533.668
Hs Code.:

Synonyms:Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

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Chemical Property of Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

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Technology Process of Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

There total 5 articles about Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1191412-83-5
rac-cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}acetic Acid

: 17994-94-4
methyl 7-aminoheptanoate hydrochloride

: 1242457-13-1
Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

Guidance literature:: With pyridine; HATU; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 613-94-5
benzoic acid hydrazide

: 1242457-13-1
Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 0.5 h / Reflux

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 100 °C

3: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

4: trifluoroacetic acid / dichloromethane

5: pyridine; HATU / N,N-dimethyl-formamide / 20 °C

With pyridine; sodium hydrogencarbonate; caesium carbonate; HATU; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 28669-17-2
2-phenyl-4H-1,3,4-oxadiazin-5(6H)-one

: 1242457-13-1
Methyl 7-[(cyclopentyl{4-[(5-oxo-2-phenyl-5,6-dihydro-4H-1,3,4-oxadiazin-4-yl)methyl]phenyl}-acetyl)amino]heptanoate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2: trifluoroacetic acid / dichloromethane

3: pyridine; HATU / N,N-dimethyl-formamide / 20 °C

With pyridine; caesium carbonate; HATU; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;