N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide

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Chemical Name:N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide
CAS No.:1586800-27-2
Molecular Formula:C₂₄H₂₆N₄O₃
Molecular Weight:418.495
Hs Code.:

Synonyms:N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide

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Chemical Property of N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide

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Technology Process of N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide

There total 2 articles about N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1586800-09-0
N-(2-(butylamino)-1-(1H-imidazol-4-yl)-2-oxoethyl)-2-iodo-N-(4-methoxybenzyl)benzamide

: 1586800-27-2
N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide

Guidance literature:: With copper(l) iodide; caesium carbonate; In dimethyl sulfoxide; at 100 ℃; for 0.5h; Sealed tube; Microwave irradiation;
DOI:10.1016/j.tetlet.2014.02.023

Reference yield:

: 2769-64-4
n-butyl isonitrile

: 88-67-5
2-Iodobenzoic acid

: 2393-23-9
4-methoxy-benzylamine

: 1586800-27-2
N-butyl-5-(4-methoxybenzyl)-6-oxo-5,6-dihydro-4H-benzo[f]imidazo[1,5-a][1,4]diazepine-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / methanol / 20 °C / Sealed tube

2: caesium carbonate; copper(l) iodide / dimethyl sulfoxide / 0.5 h / 100 °C / Sealed tube; Microwave irradiation

With copper(l) iodide; caesium carbonate; sodium sulfate; In methanol; dimethyl sulfoxide; 1: |Ugi Condensation / 2: |Ullmann Condensation;
DOI:10.1016/j.tetlet.2014.02.023