endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

Base Information

Chemical Name:endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide
CAS No.:139632-39-6
Molecular Formula:C₁₇H₂₃ClN₄O₃
Molecular Weight:366.848
Hs Code.:

Synonyms:endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

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Chemical Property of endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

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Technology Process of endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

There total 5 articles about endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139632-37-4
endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-2-methoxybenzamide

: 139632-39-6
endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

Guidance literature:: With 1,2-Dichloro-3-iodobenzene; In chloroform; at 0 ℃; for 12h;
DOI:10.1021/jm00087a003

Reference yield:

: 62726-03-8
2-methoxy-4-nitrobenzamide

: 139632-39-6
endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1,2-dichloro-ethane / 19 h / 70 °C

2: toluene; tetrahydrofuran; hexane

3: H₂ / 5percent Pd-C / acetic acid / 2 h / 28 °C / 1810.02 Torr

4: iodobenzene dichloride / CHCl₃ / 12 h / 0 °C

With 1,2-Dichloro-3-iodobenzene; hydrogen; palladium on activated charcoal; In tetrahydrofuran; hexane; chloroform; acetic acid; 1,2-dichloro-ethane; toluene;
DOI:10.1021/jm00087a003

Reference yield:

: 2-Methoxy-4-nitro-benzoyl isocyanate

: 139632-39-6
endo-N-<<(8-methyl-8-azabicyclo<3.2.1>octan-3-yl)amino>carbonyl>-4-amino-5-chloro-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene; tetrahydrofuran; hexane

2: H₂ / 5percent Pd-C / acetic acid / 2 h / 28 °C / 1810.02 Torr

3: iodobenzene dichloride / CHCl₃ / 12 h / 0 °C

With 1,2-Dichloro-3-iodobenzene; hydrogen; palladium on activated charcoal; In tetrahydrofuran; hexane; chloroform; acetic acid; toluene;
DOI:10.1021/jm00087a003