Technology Process of C62H80N6O16
There total 4 articles about C62H80N6O16 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
1,5-difluoro-2,4-dinitrobenzene; C28H40N2O6;
In
dimethyl sulfoxide;
at 20 ℃;
for 4h;
Inert atmosphere;
With
N-ethyl-N,N-diisopropylamine;
In
dimethyl sulfoxide;
at 20 ℃;
for 48h;
Inert atmosphere;
DOI:10.1021/ol500512f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h
2.1: dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere
2.2: 48 h / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen;
In
dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/ol500512f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl dichloride / chloroform / 2 h / 20 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine / chloroform / 16 h / 20 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 16 h
4.1: dimethyl sulfoxide / 4 h / 20 °C / Inert atmosphere
4.2: 48 h / 20 °C / Inert atmosphere
With
oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine;
In
chloroform; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/ol500512f