benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol)

Base Information

• Chemical Name: benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol)
• CAS No.: 1033003-02-9
• Molecular Formula: C₄₁H₆₁NO₂
• Molecular Weight: 599.941
• Mol file: 1033003-02-9.mol

Synonyms:benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol)

Chemical Property of benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol)

There total 1 articles about benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2,4-di-tert-amylphenol (120-95-6) + benzylamine (100-46-9) → benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol) (1033003-02-9)

Guidance literature:

In water; at 100 ℃; for 18h;

DOI:10.1139/V08-043

Reference yield: 98.6%

trichlorotris(tetrahydrofuran)chromium(III) (10170-68-0,16997-54-9) + benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol) (1033003-02-9) → C45H67ClCrNO3 (1610504-68-1)

Guidance literature:

benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol); With n-butyllithium; In hexane; at -78 - 20 ℃; for 2h; Schlenk technique; Inert atmosphere;

trichlorotris(tetrahydrofuran)chromium(III); In tetrahydrofuran; hexane; at -78 ℃; for 18h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c3cy01002c

Reference yield: 84.0%

ferric(III) bromide (10031-26-2) + benzylamine-N,N-bis(2-methylene-4,6-di-tert-amylphenol) (1033003-02-9) → FeBr(THF)L1 (1430322-45-4)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at -78 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.03.034

upstream raw materials:

formaldehyd

2,4-di-tert-amylphenol

benzylamine

Downstream raw materials:

FeCl(THF)L₁

FeBr(THF)L₁

C₄₅H₆₇ClCrNO₃