1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

Base Information

Chemical Name:1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester
CAS No.:145193-42-6
Molecular Formula:C₅₀H₄₅ClO₁₀
Molecular Weight:841.354
Hs Code.:

Synonyms:1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

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Chemical Property of 1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

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Technology Process of 1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

There total 3 articles about 1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.2%

: 64-17-5
ethanol

: 145193-41-5
1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure

: 145193-42-6
1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

Guidance literature:: With sulfuric acid; for 24h; Heating;

Reference yield:

: 2519-10-0
1,2,3,4,5-pentaphenylcyclopentadiene

: 145193-42-6
1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 76.8 percent / AlCl₃ / 1,2-dichloro-ethane / 1) 2 h, r.t., 2) 16-20 h, 50-60 deg C

2: 67.8 percent / KOCl / dioxane / 2 h / Ambient temperature

3: 91.2 percent / conc. H₂SO₄ / 24 h / Heating

With aluminium trichloride; potassium hypochlorite; sulfuric acid; In 1,4-dioxane; 1,2-dichloro-ethane;

Reference yield:

: 145193-37-9
1,2,3,4,5-Penta(4-acetylphenyl)-1,3-cyclopentadiene

: 145193-42-6
1-<4-<1,1',1'',1''',1''''-(5-Chloro-1,3-cyclopentadien-1,2,3,4,5-pentayl)pentakis>>benzoesaeure pentaethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 67.8 percent / KOCl / dioxane / 2 h / Ambient temperature

2: 91.2 percent / conc. H₂SO₄ / 24 h / Heating

With potassium hypochlorite; sulfuric acid; In 1,4-dioxane;