methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

Base Information

Chemical Name:methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester
CAS No.:1203905-05-8
Molecular Formula:C₁₇H₂₄BrNO₆S
Molecular Weight:450.351
Hs Code.:

Synonyms:methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

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Chemical Property of methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

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Technology Process of methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

There total 1 articles about methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1203905-03-6
methanesulfonic acid 4-allyloxy-2-bromo-3-(2-carbamoylethyl)phenyl ester

: 75-65-0
tert-butyl alcohol

: 1203905-05-8
methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

Guidance literature:: With lead(IV) tetraacetate; at 70 ℃; for 0.5h;
DOI:10.1039/b914580j

Reference yield: 94.0%

: 1203905-05-8
methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

: 1203905-07-0
[2-(6-allyloxy-2-bromo-3-hydroxyphenyl)ethyl]carbamic acid tert-butyl ester

Guidance literature:: With trimethylphenylammonium hydroxide; In 1,4-dioxane; methanol; water; at 50 - 60 ℃; for 6h;
DOI:10.1039/b914580j

Reference yield:

: 1203905-05-8
methanesulfonic acid 4-allyloxy-2-bromo-3-[(2-tert-butoxycarbonylamino)ethyl]-phenyl ester

: C₁₄H₂₀BrNO₆S

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In methanol; for 4h; Inert atmosphere;
DOI:10.1039/b914580j