nickel 5,10-diphenylporphyrin

Base Information

• Chemical Name: nickel 5,10-diphenylporphyrin
• CAS No.: 457957-32-3
• Molecular Formula: C₃₂H₂₀N₄Ni
• Molecular Weight: 519.228

Synonyms:nickel 5,10-diphenylporphyrin

Chemical Property of nickel 5,10-diphenylporphyrin

Chemical Property:

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Technology Process of nickel 5,10-diphenylporphyrin

There total 3 articles about nickel 5,10-diphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,10-diphenyltripyrrane (195381-16-9) → nickel 5,10-diphenylporphyrin (457957-32-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / chloroform; methanol / 1 h / 20 °C / Darkness

1.2: 0.67 h / 20 °C / Darkness

2.1: toluene / Reflux

With boron trifluoride diethyl etherate; In methanol; chloroform; toluene;

DOI:10.1142/S1088424617500705

Reference yield:

(1H-pyrrole-2,5-diyl)dimethanol (6249-04-3) → nickel 5,10-diphenylporphyrin (457957-32-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / chloroform; methanol / 1 h / 20 °C / Darkness

1.2: 0.67 h / 20 °C / Darkness

2.1: toluene / Reflux

With boron trifluoride diethyl etherate; In methanol; chloroform; toluene;

DOI:10.1142/S1088424617500705

Reference yield:

bis(2,4-pentanedionate)nickel(II) hydrate (120156-44-7) + 5,10-diphenylphorphyrin → nickel 5,10-diphenylporphyrin (457957-32-3)

Guidance literature:

In toluene; Reflux;

DOI:10.1142/S1088424617500705

upstream raw materials:

bis(2,4-pentanedionate)nickel(II) hydrate

5,10-diphenyltripyrrane

(1H-pyrrole-2,5-diyl)dimethanol

Downstream raw materials:

[5,10-di(n-hexyl)-15,20-diphenylporphyrinato]nickel(II)

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