2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile

Base Information

• Chemical Name: 2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile
• CAS No.: 1073973-35-9
• Molecular Formula: C₁₉H₁₈BrFN₂O
• Molecular Weight: 389.267

Synonyms:2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile

Chemical Property of 2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile

Chemical Property:

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Technology Process of 2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile

There total 1 articles about 2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-bromo-2,6-difluorobenzonitrile (123843-67-4) + (1S,2S)-2-(benzyloxy)cyclopentanamine (181657-56-7,404028-21-3,796038-32-9,181657-57-8) → 2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile (1073973-35-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 120 ℃; for 2h;

Reference yield:

3,6,6-trimethyl-6,7-dihydro-1H-indole-4(5H)-one (56008-20-9) + 2-((1S,2S)-2-(benzyloxy)-cyclopentylamino)-4-bromo-6-fluorobenzonitrile (1073973-35-9) → 2-((1S,2S)-2-(benzyloxy)cyclopentylamino)-6-fluoro-4-(3,6,6-trimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indol-1-yl)benzonitrile (1073973-63-3)

Guidance literature:

With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In 1,4-dioxane; at 0 - 100 ℃; Sealed;

upstream raw materials:

4-bromo-2,6-difluorobenzonitrile

(1S,2S)-2-(benzyloxy)cyclopentanamine

Downstream raw materials:

2-((1S,2S)-2-(benzyloxy)cyclopentylamino)-6-fluoro-4-(3,6,6-trimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indol-1-yl)benzonitrile

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