3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester

Base Information

Chemical Name:3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester
CAS No.:171255-53-1
Molecular Formula:C₂₇H₂₅ClN₂O₆
Molecular Weight:508.958
Hs Code.:

Synonyms:3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester

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Chemical Property of 3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester

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Technology Process of 3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester

There total 2 articles about 3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1489-06-1
2,3-diphenyl-5,6-dihydropyrazine

: 171255-53-1
3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Zn / 110 °C

2: 94 percent / dimethyldioxirane / acetone / 0 °C

3: CDCl₃ / -20 °C

With 3,3-dimethyldioxirane; zinc; In chloroform-d1; acetone;
DOI:10.1021/ja00143a011

Reference yield:

: 32174-85-9
1,4-diacetyl-2,3-diphenyl-1,4,5,6-tetrahydropyrazine

: 171255-53-1
3-Chloro-benzenecarboperoxoic acid 1,4-diacetyl-3-hydroxy-2,3-diphenyl-piperazin-2-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / dimethyldioxirane / acetone / 0 °C

2: CDCl₃ / -20 °C

With 3,3-dimethyldioxirane; In chloroform-d1; acetone;
DOI:10.1021/ja00143a011