(2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate

Base Information

Chemical Name:(2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate
CAS No.:98920-46-8
Molecular Formula:C₁₇H₂₄O₉
Molecular Weight:372.372
Hs Code.:

Synonyms:(2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate

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Chemical Property of (2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate

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Technology Process of (2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate

There total 2 articles about (2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-24-7
acetic anhydride

: 82659-55-0
3-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosyl)prop-1-ene

: 53263-18-6,82659-53-8,98920-46-8,98920-48-0,98920-49-1,103773-87-1,98920-44-6
allyl 2,3,4,6-tetra-O-acetyl-α-D-galactopyranoside

: 3-(3',4',6'-tri-O-acetyl-2'-O-benzyl-α-D-galactopyranosyl)-1-propene

Guidance literature:: 3-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosyl)prop-1-ene; With boron trichloride; In dichloromethane; at -78 ℃; for 2h;

acetic anhydride; In pyridine; at 20 ℃; for 15h;
DOI:10.1016/j.carres.2004.12.001

Reference yield:

: 25878-60-8
D-galactose pentaacetate

: 762-72-1
allyl-trimethyl-silane

: 10343-15-4,39698-55-0,78730-32-2,119111-31-8,119111-32-9,54400-76-9
allyl-2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

: 53263-18-6,82659-53-8,98920-46-8,98920-48-0,98920-49-1,103773-87-1,98920-44-6
allyl 2,3,4,6-tetra-O-acetyl-α-D-galactopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In nitromethane; for 27h; Inert atmosphere;
DOI:10.1021/ja806284x

Reference yield: 98.0%

: 2113-51-1
2-iodobiphenyl

: 98920-46-8
(2R,3R,4R,5R,6R)-2-(acetoxymethyl)-6-allyltetrahydro-2H-pyran-3,4,5-triyl triacetate

: C₂₉H₃₂O₉

Guidance literature:: With tetrabutylammomium bromide; palladium diacetate; sodium hydrogencarbonate; In N,N-dimethyl-formamide; Inert atmosphere; Heating;
DOI:10.3390/molecules22071101